Mass spectrometry in materials synthesis
Mass spectrometry in materials synthesis
复制标题
材料合成中的质谱分析
DOI:
10.1016/j.trac.2023.117010
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发表时间:
2023
期刊:
影响因子:
--
通讯作者:
Cooks, R. Graham
中科院分区:
文献类型:
--
作者:
Ghosh, Jyotirmoy;Cooks, R. Graham
Mass spectrometry (MS), a century-old analytical technique, is now emerging as a preparative method. Electrospray deposition (ESD) of charged droplets generated by electrospray ionization (ESI) is an efficient means of forming nanomaterials, including catalysts. Much higher chemical specificity in the modification of surfaces can be achieved using mass-analyzed ions and performing ion soft landing (SL) although the low ion currents make this vacuum-based method slow. MS-based synthesis by either ESD or SL has considerable advantages over traditional approaches, providing control over the chemical identity, morphology, thickness, and surface patterning of materials while avoiding additives, ligands, and reducing agents. These MS-based methodologies are expected to provide considerable opportunities to optimize catalysts, prepare electronic devices or generate pure biopolymers.
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