3D-printed system optimizing dissolution of hyperpolarized gaseous species for micro-sized NMR

3D-printed system optimizing dissolution of hyperpolarized gaseous species for micro-sized NMR
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DOI:
10.1039/c5lc00193e
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发表时间:
2015-01-01
期刊:
影响因子:
6.1
通讯作者:
Berthault, P.
Berthault, P.
中科院分区:
工程技术1区
文献类型:
--
作者:
Causier, A.;Carret, G.;Berthault, P.

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溶解的超极化物质在液体中的利益核磁共振往往受到阻碍的存在下,降低了场的均匀性的气泡。在这里,一个由气泡泵和微型NMR单元组成的设备都安装在NMR磁体的窄孔内,通过3D打印构建。用超极化氙进行的NMR-129实验揭示了气体在水中的高度和均匀的溶解。
Dissolution of hyperpolarized species in liquids of interest for NMR is often hampered by the presence of bubbles that degrade the field homogeneity. Here a device composed of a bubble pump and a miniaturized NMR cell both fitted inside the narrow bore of an NMR magnet is built by 3D printing. Xe-129 NMR experiments performed with hyperpolarized xenon reveal high and homogeneous dissolution of the gas in water.