Preparation and characterization of Fe3O4-CNTs magnetic nanocomposites for potential application in functional magnetic printing ink

Preparation and characterization of Fe3O4-CNTs magnetic nanocomposites for potential application in functional magnetic printing ink
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Fe3O4-CNTs磁性纳米复合材料的制备和表征在功能性磁性印刷油墨中的潜在应用

DOI:
10.1016/j.compositesb.2015.11.041
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发表时间:
2016-03
期刊:
Composites Part B Engineering
影响因子:
--
通讯作者:
Wanqing Lei
Wanqing Lei
中科院分区:
其他
文献类型:
--
作者:
Xing Zhou;Changqing Fang;Yan Li;Ningli An;Wanqing Lei

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本文采用原位水热法将Fe 3 O 4纳米粒子接枝到多壁碳纳米管(CNTs)上,制备了磁性碳纳米管-Fe 3 O 4-CNTs纳米复合材料。采用傅里叶变换红外光谱(FT-IR)、拉曼光谱(Raman)、透射电子显微镜(TEM)、扫描电子显微镜(SEM)、X射线衍射(XRD)和振动样品磁强计(VSM)对所制备的Fe 3 O 4-CNTs纳米复合材料进行了表征。结果表明,粒径在20-50 nm之间的Fe 3 O 4纳米粒子与碳纳米管之间具有较强的磁吸附,复合材料具有较高的磁饱和值,即较高的磁吸附力。并将该纳米复合材料通过物理共混法制备了磁性印刷油墨。通过扫描电镜和振动扫描电镜对油墨膜进行了检测,结果表明,该磁性油墨具有明显的磁附着力,干燥后的油墨膜光滑,适合于印刷行业。
This paper presents the synthesis of magnetic carbon nanotube, Fe3O4-CNTs nanocomposites, in which Fe3O4nanoparticles were grafted to multi-walled carbon nanotube (CNTs) by thein situhydrothermal method. The prepared Fe3O4-CNTs nanocomposites were characterized by Fourier transform infrared spectroscopy (FT-IR), Raman, transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and vibrating sample magetiometer (VSM). It was found that the Fe3O4nanoparticles with the size of 20–50 nm had been attached to the CNTs strongly and the nanocomposites exhibited high magnetic saturation value, namely a high magnetic attachment force. Moreover, the nanocomposites were used to prepare magnetic printing ink via physical blending process. The ink film was detected by SEM and VSM, demonstrating that the magnetic ink which holds significant magnetic attachment force and drying smooth film is suitable for the printing industry.
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