Development of a Method for the Analysis of Four Plant Growth Regulators (PGRs) Residues in Soybean Sprouts and Mung Bean Sprouts by Liquid Chromatography–Tandem Mass Spectrometry

Development of a Method for the Analysis of Four Plant Growth Regulators (PGRs) Residues in Soybean Sprouts and Mung Bean Sprouts by Liquid Chromatography–Tandem Mass Spectrometry
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DOI:
10.1007/s00128-012-0739-z
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发表时间:
2012-07
影响因子:
2.7
通讯作者:
F. Zhang;Pengyue Zhao;W. Shan;Yong Gong;Qiu Jian;C. Pan
F. Zhang;Pengyue Zhao;W. Shan;Yong Gong;Qiu Jian;C. Pan
中科院分区:
环境科学与生态学4区
文献类型:
--
作者:
F. Zhang;Pengyue Zhao;W. Shan;Yong Gong;Qiu Jian;C. Pan

文献摘要

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A method has been developed for the simultaneous determination of four plant growth regulators (PGRs) residues in soybean sprouts and mung bean sprouts. The sample preparation procedure was based on a QuEChERS method. The method showed excellent linearity (r2≥ 0.9985) and precision (RSDs ≤ 13.0 %). Average recoveries of four PGRs ranged between 74.9 % and 106.3 % at spiking levels 0.05, 0.5 and 1 mg kg−1. The LODs and LOQs were in the ranges of 0.27–9.3 μg kg−1and 0.90–31 μg kg−1, respectively. The procedure was applied to 18 bean sprout samples, and benzyladenine was found in some of the analyzed samples.