Defect Recovery in Severely Deformed Ferrite Lamellae During Annealing and Its Impact on the Softening of Cold-Drawn Pearlitic Steel Wires

Defect Recovery in Severely Deformed Ferrite Lamellae During Annealing and Its Impact on the Softening of Cold-Drawn Pearlitic Steel Wires
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严重变形铁素体片层退火过程中的缺陷恢复及其对冷拉珠光体钢丝软化的影响

DOI:
10.1007/s11661-015-3263-z
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发表时间:
2016-02-01
影响因子:
2.8
通讯作者:
Kirchheim, R.
Kirchheim, R.
中科院分区:
材料科学2区
文献类型:
--
作者:
Chen, Y. Z.;Csiszar, G.;Kirchheim, R.

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Cold-drawn pearlitic steel wires with a drawing true strain of 3 were annealed at temperatures (T (ann)) ranging from 423 K to 723 K (150 A degrees C to 450 A degrees C) with an interval of 50 K. Recovery of the lattice defects in the severely deformed ferrite lamellae were characterized by means of high-energy X-ray diffraction and positron annihilation techniques (including positron annihilation spectroscopy and coincidence Doppler broadening spectroscopy). Accordingly, the impact of defect recovery on the softening of the annealed wires was investigated. It is found that at low temperatures [T (ann) a parts per thousand currency sign 523 K (250 A degrees C)], the recovery of the lattice defects in ferrite lamellae is dominated by the agglomeration and annihilation of vacancy clusters, while at T (ann) > 523 K (250 A degrees C), the recovery process is controlled by the annihilation of dislocations. Further analyses on the softening of the annealed wires indicate that the evolutions of dislocation density and concentration of vacancy clusters, and the strain age hardening in ferrite lamellae play important roles in changing the strength of the wires. The strain aging hardening leads to a maximum strength at 473 K (150 A degrees C). Above 523 K (250 A degrees C), the annihilations of vacancy clusters and dislocations in ferrite lamellae cause a continuous softening of the wires, where the decrease in dislocation density plays a major role.