Preparation of MnO2 nanoparticles by directly mixing potassium permanganate and polyelectrolyte aqueous solutions

Preparation of MnO2 nanoparticles by directly mixing potassium permanganate and polyelectrolyte aqueous solutions
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DOI:
10.1016/j.matlet.2006.07.165
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发表时间:
2007-04-01
期刊:
影响因子:
3
通讯作者:
Luo, Yonglan
Luo, Yonglan
中科院分区:
材料科学3区
文献类型:
--
作者:
Luo, Yonglan

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采用高锰酸钾和硼砂水溶液直接混合的方法,以硼砂作为还原剂和保护剂,制备了稳定性良好的MnO 2纳米粒子。通过透射电子显微镜(TEM)和X射线光电子能谱(XPS)对纳米粒子进行了表征,并通过原位紫外-可见光谱进一步跟踪了其生长动力学。(c)2006 Elsevier B. V.保留所有权利。
Well-stable MnO2 nanoparticles were prepared by directly mixing potassium permanganate and polyelectrolyte aqueous solutions, with the use of polyelectrolyte to serve both as a reducing agent and a protective agent. Such nanoparticles were characterized by transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS), and their growth kinetics was further traced by in situ UV-vis spectra. (c) 2006 Elsevier B.V. All rights reserved.