MILD AND CONVENIENT OXIDATION PROCEDURE FOR CONVERSION OF ORGANOBORANES TO CORRESPONDING ALCOHOLS
MILD AND CONVENIENT OXIDATION PROCEDURE FOR CONVERSION OF ORGANOBORANES TO CORRESPONDING ALCOHOLS
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DOI：
10.1021/jo00900a022
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发表时间：
1975-01-01
影响因子：
3.6
通讯作者：
HEDGECOCK, HC
中科院分区：
文献类型：
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作者：
KABALKA, GW;HEDGECOCK, HC
(7)如果将乙醇置于玻璃管（2.5英尺× 55毫米）中，碱悬浮在液体的上三分之一处，则165克KOH颗粒将迅速溶解在600毫升乙醇中。溶液的时间从6小时（在烧杯或锥形瓶中）减少到在玻璃管中的30分钟。
(7) A 165-g portion of KOH pellets will dissolve rapidly In 600 ml of ethanol if the alcohol is placed in a glass tube (2.5 ft X 55 mm) and the alkali sus-pended in the upper third of the liquid. The time of solution Is reduced from 6 hr (In a beaker or erlenmeyer) to 30 min in the glass tube.