Implementation of Nanoscale Secondary-Ion Mass Spectrometry Analyses: Application to Ni-Based Superalloys

Implementation of Nanoscale Secondary-Ion Mass Spectrometry Analyses: Application to Ni-Based Superalloys
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DOI:
10.1002/pssa.202100414
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发表时间:
2021-12-20
影响因子:
2
通讯作者:
Bozzolo, Nathalie
Bozzolo, Nathalie
中科院分区:
材料科学4区
文献类型:
--
作者:
Almoric, Jean;Durand, Malik;Bozzolo, Nathalie

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Secondary-ion mass spectrometry (SIMS) is probably the most widely used chemical analysis technique in semiconductor science and in metallurgy because of its ultimate sensitivity to all elements and in particular to light elements providing semiquantitative information on the depth distribution of elements, for instance, doping elements (i.e., B, H), contaminants (i.e., C and O), chemical gradients, and segregation in thin films and at interfaces, etc. With the size shrinking of systems, high-resolution 3D chemical imaging is becoming a prerequisite for the development of new materials at the nanoscale and for the deep understanding of the correlation between their properties and functionalities. Herein, the development of an innovative analytical SIMS implemented in a focused ion beam (FIB) (using Ga source)/scanning electron microscope (SEM) is reported. The equipment enables to give elemental chemical mapping at very high resolution (