Single-crystal structure determination from microcrystalline powders (~5 μm) by an orientation attachment mountable on an In-house X-ray diffractometer
Single-crystal structure determination from microcrystalline powders (~5 μm) by an orientation attachment mountable on an In-house X-ray diffractometer
复制标题
通过安装在内部 X 射线衍射仪上的定向附件测定微晶粉末 (~5 μm) 的单晶结构
DOI：
10.1039/c5ce02307f
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发表时间：
2016
期刊：
影响因子：
3.1
通讯作者：
and Tsunehisa Kimura
中科院分区：
文献类型：
--
作者：
Chiaki Tsuboi;Kazuaki Aburaya;Fumiko Kimura;Masataka Maeyama;and Tsunehisa Kimura
提出了一种能够实现微晶粉末单晶X射线衍射的X射线装置。单晶衍射数据是在原位获得的，并使用传统的计算机软件进行分析，以确定微晶的晶体结构。使用L-丙氨酸微晶（1.5 μm）证明了附着的性能。
An X-ray attachment that can realize single-crystal X-ray diffraction patterns from microcrystalline powders is proposed. Single-crystal diffraction data are acquired in situ and analyzed using conventional computer software to determine the crystal structure of the microcrystals. The performance of the attachment is demonstrated using L-alanine microcrystals (∼5 μm).