Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant
Easy Preparation of (Diacetoxyiodo)arenes from Iodoarenes with Sodium Percarbonate as the Oxidant
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DOI：
10.3390/71100806
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发表时间：
2002-11-30
期刊：
影响因子：
--
通讯作者：
Skulski L
中科院分区：
文献类型：
--
作者：
Zielinska A;Skulski L
本文报道了从碘代芳烃ArI出发，简便而有效地制备近纯的二乙酰氧基碘代芳烃ArI（OAc）2的方法。在大多数情况下，由此获得的无色粗产物不需要进一步纯化，即，通过重结晶。作为一个实例，如此制备的PhI（OAc）2的纯度为99%（通过碘量法）。
Easy and effective preparations of nearly pure (diacetoxyiodo)arenes, ArI(OAc)2, from iodoarenes, ArI, are reported. In most cases the crude colorless products thus obtained need not be further purified, i.e., by recrystallization. As an example, the PhI(OAc)2 thus prepared was 99% pure (by iodometry).
影响因子：
4.6
作者：
Skulski, L
通讯作者：
Skulski, L