Synthesis and characterization of nano-sized nickel ferrites from fly ash for catalytic oxidation of CO

Synthesis and characterization of nano-sized nickel ferrites from fly ash for catalytic oxidation of CO
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DOI:
10.1016/j.matchemphys.2005.05.028
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发表时间:
2005-12-15
影响因子:
4.6
通讯作者:
Fouad, OA
Fouad, OA
中科院分区:
材料科学3区
文献类型:
--
作者:
Rashad, MM;Fouad, OA

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以粉煤灰为原料,采用共沉淀法合成了纳米铁酸镍粉体。X射线衍射分析表明,纯的结晶镍铁氧体NiFe,04相可以通过在所研究的pH范围(从7(中性)到12(高碱性))中在>800 ° C的温度下热处理前体120分钟来获得。在500摄氏度的温度范围内
Nano-sized nickel ferrite powders have been synthesized from fly ash via a chemical synthesis route, co-precipitation method. X-ray diffraction analyses showed that pure crystalline nickel ferrite, NiFe,04, phase can be obtained by thermal treatment of the precursors at temperature >800 degrees C for 120 min in the studied pH range, from 7 (neutral) to 12 (highly alkaline). In the temperature range of 500 degrees C