Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples

Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples
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与多相催化剂样品的非弹性中子散射测量采集相关的样品环境问题

DOI:
10.1088/1742-6596/554/1/012005
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发表时间:
2014
期刊:
Conference Series
影响因子:
--
通讯作者:
Warringham R
Warringham R
中科院分区:
--
文献类型:
--
作者:
Warringham R

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改进建立的样品处理问题与非弹性中子散射(INS)光谱的非均相催化剂样品的收购进行了说明。这涉及反应器的修改和气体处理设备的改进。后者包括提供实验室空间和通风设施,以适应日益广泛的催化样品的检测。INS测量CO加氢超过铁基费托催化剂使用MARI光谱仪记录,以说明新的安排的适用性。
Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements.
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