In-situ investigation and effect of additives on low temperature aqueous chemical synthesis of Bi2Te3 nanocapsules

In-situ investigation and effect of additives on low temperature aqueous chemical synthesis of Bi2Te3 nanocapsules
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DOI:
10.1039/b500759c
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发表时间:
2005-04
影响因子:
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通讯作者:
Xinbing Zhao;T. Sun;T. Zhu;J. Tu
Xinbing Zhao;T. Sun;T. Zhu;J. Tu
中科院分区:
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文献类型:
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作者:
Xinbing Zhao;T. Sun;T. Zhu;J. Tu

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在65℃的开放体系中,用低温水化学方法成功地合成了直径50~200 nm、长度100~800 nm的Bi2Te3中空结构纳米胶囊。管壁厚度约为6 nm,法向平行于Bi2Te3晶格的c轴。对合成过程中的化学反应和纳米胶囊的形成进行了原位研究。
Bi2Te3 nanocapsules with hollow structure have been successfully synthesized by a low temperature aqueous chemical route in an open system at 65 °C. The nanocapsules are 50–200 nm in diameter and 100–800 nm in length. The tube walls have a thickness of about 6 nm with the normal parallel to the c-axis of the Bi2Te3 crystal lattice. Chemical reactions during synthesis and the formation of the nanocapsules were investigated in-situ.