Use of silver nitrate impregnated silica cartridges in the separation of kahweol and cafestol esters by preparative liquid chromatography.
Use of silver nitrate impregnated silica cartridges in the separation of kahweol and cafestol esters by preparative liquid chromatography.
复制标题
使用硝酸银浸渍的硅胶柱通过制备型液相色谱分离咖啡醇和咖啡醇酯。
DOI：
10.1016/s0021-9673(01)87421-5
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发表时间：
1985
期刊：
影响因子：
--
通讯作者：
Wattenberg,LW
中科院分区：
文献类型：
--
作者：
Lam,LK;Yee,C;Chung,A;Wattenberg,LW
A 20.0-g amount of silver nitrate (99.9+% pure, Alfa Products) was dissolved in 40 ml distilled water. This 50% silver nitrate solution was added slowly to 180 g Kieselgel60 silica gel (40-63 pm particle size, Merck reagent) and hand mixed during this addition. The silver nitrat~ ilica mixture was then placed in a plastic container and mixed for 0.5 h using a PTFE stirrer blade, a heavy duty glass stirrer shaft and a Talboy T-Line laboratory stirrer. The silver nitrate-silica mixture was then spread in a thin layer on stainless-steel trays and dried in an oven maintained at 105-120 C for 17 min to remove the water.
