Characterization of h-WO3 nanorods synthesized by hydrothermal process
Characterization of h-WO3 nanorods synthesized by hydrothermal process
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DOI：
10.1016/j.poly.2010.02.025
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发表时间：
2010-05-10
期刊：
影响因子：
2.6
通讯作者：
Gharbi, N.
中科院分区：
文献类型：
--
作者：
Salmaoui, S.;Sediri, F.;Gharbi, N.
以Na 2 WO 4中心点2 H（2）O为钨源，苯胺和硫酸钠为模板剂，采用水热法合成了六方钨氧化物纳米棒。采用X射线衍射（XRD）、扫描电子显微镜（SEM）、透射电子显微镜（TEM）、高分辨透射电子显微镜（HRTEM）、傅里叶变换红外光谱（FTIR）和拉曼光谱等技术对纳米棒的结构、形貌和组成进行了表征。纳米棒的长度可达5 μ m，直径为50-70 nm。(C)2010爱思唯尔有限公司保留所有权利。
Hexagonal tungsten oxide nanorods have been synthesized by hydrothermal strategy using Na2WO4 center dot 2H(2)O as tungsten source, aniline and sulfate sodium as structure-directing templates. Techniques X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanorods. The h-WO3 nanorods are up to 5 mu m in length, and 50-70 nm in diameter. (C) 2010 Elsevier Ltd. All rights reserved.