Double-sided laser heating system for in situ high pressure–high temperature monochromatic x-ray diffraction at the esrf

Double-sided laser heating system for in situ high pressure–high temperature monochromatic x-ray diffraction at the esrf
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ESRF 原位高压高温单色 X 射线衍射的双面激光加热系统

DOI:
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发表时间:
2005
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影响因子:
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通讯作者:
P. Loubeyre
P. Loubeyre
中科院分区:
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文献类型:
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作者:
E. Schultz;M. Mezouar;W. Crichton;S. Bauchau;G. Blattmann;D. Andrault;G. Fiquet;R. Boehler;N. Rambert;B. Sitaud;P. Loubeyre

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在欧洲同步辐射装置(ESRF)的ID27光束线上,研制了一种用于高温高压单色X射线衍射的新型双面激光加热系统。该系统的主要组成部分,包括优化的聚焦光学产生一个大的和均匀的加热区域,优化的反射镜光学温度测量和一个国家的最先进的衍射设置进行了详细描述。本文介绍了在高压和高温下收集的钨和铁的初步数据。
A new double-sided laser heating system optimized for monochromatic X-ray diffraction at high pressure and high temperature has been developed at beamline ID27 of the European Synchrotron Radiation Facility (ESRF). The main components of this system including optimized focusing optics to produce a large and homogenous heated area, optimized mirror optics for temperature measurements and a state-of-the-art diffraction setup are described in details. Preliminary data collected at high pressure and high temperature on tungsten and iron are presented.