Preparation of porous hydroxyapatite ceramics containing mullite by reaction sintering of clay, alumina and hydroxyapatite

Preparation of porous hydroxyapatite ceramics containing mullite by reaction sintering of clay, alumina and hydroxyapatite
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DOI:
10.1016/j.ceramint.2011.02.020
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发表时间:
2011-09-01
影响因子:
5.2
通讯作者:
Nemati, R.
Nemati, R.
中科院分区:
材料科学1区
文献类型:
--
作者:
Ebadzadeh, T.;Behnamghader, A.;Nemati, R.

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在纯羟基磷灰石存在下,粘土和氧化铝在1150 ℃至1350 ℃下反应烧结,获得含莫来石的多孔羟基磷灰石陶瓷。XRD结果表明,加入莫来石后,羟基磷灰石分解为TCP。在含有10重量%的样品中检测到羟基磷灰石、β-TCP和莫来石。莫来石较多,在1150 ℃和1250 ℃下烧结2 h。气孔率随莫来石的加入而增加,随烧结温度的升高而降低。最高的孔隙率含量是在含有30重量%莫来石在所有烧结温度。(C)2011 Elsevier Ltd和Techna Group S.r.l. All rights reserved.
Porous hydroxyapatite ceramics containing mullite have been obtained from reaction sintering at 1150 degrees to 1350 degrees C of clay and alumina in the presence of pure hydroxyapatite. XRD results showed that hydroxyapatite decomposes to TCP by adding mullite. Hydroxyapatite, beta-TCP and mullite were detected in samples containing 10 wt.% and more mullite, sintered at 1150 degrees and 1250 degrees C for 2 h. Porosity amount increased by adding mullite and decreased by increasing sintering temperature. The highest porosity content was in samples containing 30 wt.% mullite at all sintering temperatures. (C) 2011 Elsevier Ltd and Techna Group S.r.l. All rights reserved.