Growth of Single-Crystalline KNbO 3 Nanostructures

Growth of Single-Crystalline KNbO 3 Nanostructures
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单晶 KNbO 3 纳米结构的生长

DOI:
10.1002/chin.200615221
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发表时间:
2006
影响因子:
3.3
通讯作者:
L. Forró
L. Forró
中科院分区:
化学3区
文献类型:
--
作者:
A. Magrez;E. Vasco;J. Seo;C. Dieker;N. Setter;L. Forró

文献摘要

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该通信报告的高度均匀的KNbO 3纳米线的生长表现出约60 nm的窄直径分布和长-宽比高达100。纳米线是通过水热路线制备的,这使得简单的克级生产成为可能。通过改变温度-压力条件和起始混合物的组成,对合成的纳米线的形态和化学特征进行了系统的研究。结果表明,高度均匀的单晶纳米线形成在一个狭窄的窗口内的三元相图的KOH-Nb 2 O 5-H2O。
This communication reports on the growth of highly uniform KNbO3nanowires exhibiting a narrow diameter distribution around 60 nm and a length-to-width ratio up to 100. The nanowires were prepared by a hydrothermal route, which enables simple, gram-scale production. A systematic study of the synthesized nanowires in terms of the morphological and chemical characteristics was carried out by varying the temperature−pressure conditions and the composition of the starting mixture. The results indicate that highly uniform single-crystalline nanowires form within a narrow window of the ternary phase diagram of KOH−Nb2O5−H2O.