Double-quantum 19F-19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides.

Double-quantum 19F-19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides.
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DOI:
10.1039/b914468d
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发表时间:
2009-11
期刊:
Physical chemistry chemical physics : PCCP
影响因子:
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通讯作者:
Qiang Wang;Bingwen Hu;F. Fayon;J. Trébosc;C. Legein;O. Lafon;F. Deng;J. Amoureux
Qiang Wang;Bingwen Hu;F. Fayon;J. Trébosc;C. Legein;O. Lafon;F. Deng;J. Amoureux
中科院分区:
其他
文献类型:
--
作者:
Qiang Wang;Bingwen Hu;F. Fayon;J. Trébosc;C. Legein;O. Lafon;F. Deng;J. Amoureux

文献摘要

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介绍了一种对化学位移具有较强鲁棒性的宽带偶极重耦合方法,用于在强磁场和超快幻角旋转(>60 kHz)下观察氟铝酸盐中的(19)F-(19)F近邻。
A broadband dipolar recoupling method robust to chemical shift is introduced to observe (19)F-(19)F proximities in fluoroaluminates in high magnetic field and at ultra-fast magic angle spinning (>60 kHz).