Synthesis and characterization of Fe-containing biphasic calcium phosphate ceramics
Synthesis and characterization of Fe-containing biphasic calcium phosphate ceramics
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DOI:
10.1007/s41779-018-0245-9
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发表时间:
2018-08
影响因子:
1.9
通讯作者:
O. Kaygili
中科院分区:
文献类型:
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作者:
O. Kaygili
Three biphasic calcium phosphate (BCP) ceramics with various Fe contents (e.g., 0.66, 1.32, and 1.98 at.%) were prepared using wet chemical synthesis. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, differential thermal analysis (DTA), thermogravimetric analysis (TG), scanning electron microscopy (SEM), and energy dispersive X-ray (EDX) spectroscopy techniques were used to characterize the as-prepared BCPs. The DTA and TG results show that the as-prepared samples are thermally stable. The addition of Fe affects significantly the lattice parameters, unit cell volume, and morphology. The EDX data confirm the introduction of Fe.