Effect of forced-air cooling on the microstructure and age-hardening response of extruded Mg-Gd-Y-Zn-Zr alloy full with LPSO lamella

Effect of forced-air cooling on the microstructure and age-hardening response of extruded Mg-Gd-Y-Zn-Zr alloy full with LPSO lamella
复制标题

强制风冷对全LPSO片层挤压Mg-Gd-Y-Zn-Zr合金显微组织和时效硬化响应的影响

DOI:
10.1016/j.jmst.2020.09.020
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发表时间:
2020-09
影响因子:
10.9
通讯作者:
Fan G. H.
Fan G. H.
中科院分区:
材料科学1区
文献类型:
--
作者:
Wu S. Z.;Nakata T.;Tang G. Z.;Xu C.;Wang X. J.;Li X. W.;Qiao X. G.;Zheng M. Y.;Geng L.;Kamado S.;Fan G. H.

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本文对含有片状长周期有序相(LPSO)的均匀化Mg-8.2Gd-3.8Y-1.0Zn-0.4Zr(wt.%)合金在常压下进行了热挤压和强制空气冷却,研究了强迫空气冷却对合金组织和时效硬化响应的影响。结果表明,与挤压样品在大气中冷却相比,强制风冷限制了动态再结晶(DRX),使动态再结晶(DRXed)晶粒度更细,基面织构更强,位错密度更高。此外,强风冷却促进了非再结晶区的动态析出,促进了未再结晶区间距较小的片状LPSO相和γ‘相的形成,对时效过程中β’相的析出有一定的抑制作用。经峰时效处理后,经强制风冷的挤压试样具有优良的拉伸性能,拉伸屈服强度为439 Mpa,极限拉伸强度为493 Mpa,断裂伸长率为18.6%。
The homogenized Mg-8.2Gd-3.8Y-1.0Zn-0.4 Zr (wt.%) alloy full of plate-shaped long period stacking ordered (LPSO) phases was hot extruded in the atmosphere and cooled by the forced-air, then the effect of forced-air cooling on the microstructure and age-hardening response of the alloy was investigated in this work. The results show that in comparison with the extruded sample cooling in the atmosphere, the forced-air cooling restricts dynamic recrystallization (DRX) and brings about finer dynamic recrystallized (DRXed) grain size, stronger basal texture and higher dislocation density. Furthermore, the forced-air cooling promotes the dynamic precipitation in the DRXed regions and facilitates formation of plate-shaped LPSO phases and γ′ phases with smaller interspacing in the unrecrystallized (unDRXed) regions, then slightly restricts the precipitation of β′ phases during aging. After peak-ageing treatment, the extruded sample with forced-air cooling shows superior tensile properties with a tensile yield strength of 439 MPa, an ultimate tensile strength of 493 MPa, and elongation to failure of 18.6 %.
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