Photocatalytic hydroxylation of arylboronic acids using continuous flow reactors

Photocatalytic hydroxylation of arylboronic acids using continuous flow reactors
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DOI：
10.1039/c4ra15588b
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发表时间：
2015
期刊：
RSC Advances
影响因子：
3.9
通讯作者：
Inès G. T. M. Penders;Zacharias Amara;Raphael Horvath;K. Rossen;M. Poliakoff;M. George
Inès G. T. M. Penders;Zacharias Amara;Raphael Horvath;K. Rossen;M. Poliakoff;M. George
中科院分区：
化学3区
文献类型：
--
作者：
Inès G. T. M. Penders;Zacharias Amara;Raphael Horvath;K. Rossen;M. Poliakoff;M. George

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采用连续流动光催化反应器和白色LED对单取代和双取代芳基硼酸光催化氧化合成苯酚进行了研究。EtOH-H2O溶剂系统在2 MPa下加速转化;而在大气压下的反应允许适度有效的去对称化。
The photocatalytic oxidation of mono- and di-substituted arylboronic acids to phenols has been investigated using a continuous flow photoreactor fitted with white LEDs. An EtOH–H2O solvent system accelerated conversion at 2 MPa; whereas reactions at atmospheric pressure allowed for moderately efficient desymmetrisation.