Volatile chemicals identified in extracts from leaves of Japanese mugwort (Artemisia princeps pamp.).
Volatile chemicals identified in extracts from leaves of Japanese mugwort (Artemisia princeps pamp.).
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艾蒿（Artemisia Princeps pamp.）叶子提取物中鉴定出挥发性化学物质。
DOI：
10.1021/jf0001738
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发表时间：
2000
影响因子：
6.1
通讯作者：
T. Shibamoto
中科院分区：
文献类型：
--
作者：
K. Umano;Y. Hagi;K. Nakahara;A. Shoji;T. Shibamoto
使用两种方法从艾蒿（Artemisia Princeps Pamp.）叶中提取提取物：减压蒸汽蒸馏，然后二氯甲烷萃取（DRP）和同时净化萃取（SPSE）。使用气相色谱 (GC) 和气相色谱-质谱 (GC-MS) 两种方法获得的提取物中总共鉴定出 192 种挥发性化学物质。其中包括47种单萜（氧化单萜）、26种芳香族化合物、19种脂肪族酯、18种脂肪醇、17种单萜（烃类单萜）、17种倍半萜（烃类倍半萜）、13种倍半萜（氧化倍半萜）、12种脂肪醛、8种脂肪烃、7 种脂肪酮和 9 种杂化合物。 DRP 提取物的主要挥发性成分为冰片 (10.27 ppm)、α-侧柏酮 (3.49 ppm)、艾蒿醇 (2.17 ppm)、马鞭草酮 (1.85 ppm)、yomogi 醇 (1.50 ppm) 和 germacren-4-ol (1.43 ppm)。 SPSE 提取物的主要挥发性成分为 1,8-桉树脑 (8.12 ppm)、醋酸蒿 (4.22 ppm)、α-侧柏酮 (3.20 ppm)、β-石竹烯 (2.39 ppm)、醋酸冰片酯 (2.05 ppm)、冰片 (1.80 ppm) 和反式 β-法呢烯 (1. 78 ppm)。
Extracts from leaves of Japanese mugwort (Artemisia princeps Pamp.) were obtained using two methods: steam distillation under reduced pressure followed by dichloromethane extraction (DRP) and simultaneous purging and extraction (SPSE). A total of 192 volatile chemicals were identified in the extracts obtained by both methods using gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS). They included 47 monoterpenoids (oxygenated monoterpenes), 26 aromatic compounds, 19 aliphatic esters, 18 aliphatic alcohols, 17 monoterpenes (hydrocarbon monoterpenes), 17 sesquiterpenes (hydrocarbon sesquiterpenes), 13 sesquiterpenoids (oxygenated sesquiterpenes), 12 aliphatic aldehydes, 8 aliphatic hydrocarbons, 7 aliphatic ketones, and 9 miscellaneous compounds. The major volatile constituents of the extract by DRP were borneol (10.27 ppm), alpha-thujone (3.49 ppm), artemisia alcohol (2.17 ppm), verbenone (1.85 ppm), yomogi alcohol (1.50 ppm), and germacren-4-ol (1.43 ppm). The major volatile constituents of the extract by SPSE were 1,8-cineole (8.12 ppm), artemisia acetate (4.22 ppm), alpha-thujone (3.20 ppm), beta-caryophyllene (2.39 ppm), bornyl acetate (2.05 ppm), borneol (1.80 ppm), and trans-beta-farnesene (1. 78 ppm).