GLUCOSAMINE OLIGOMERS .1. PREPARATION AND CHARACTERIZATION

GLUCOSAMINE OLIGOMERS .1. PREPARATION AND CHARACTERIZATION
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DOI:
10.1016/0141-8130(89)90023-8
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发表时间:
1989-10-01
影响因子:
8.2
通讯作者:
CARTIER, N
CARTIER, N
中科院分区:
化学1区
文献类型:
--
作者:
DOMARD, A;CARTIER, N

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壳聚糖在热浓HCl中的水解导致壳寡糖[β-(1 → 4)连接的2-氨基-2-脱氧-D-葡萄糖]。研究了分布的时间依赖性。这些水解产物的空间排阻色谱条件的方便选择允许分离的前15个低聚物和高达DP = 40的馏分。
Hydrolysis of chitosan in hot concentrated HCl led to chito-oligosaccharides [.beta.-(1.fwdarw.4) linked 2-amino-2-deoxy-D-glucose]. The time dependence of the distribution was studied. A convenient choice of the conditions for steric exclusion chromatography of these hydrolysates allowed the separation of the first 15 oligomers and of fractions up to DP = 40.