DETECTION OF EPOXIDES WITH 4-(PARA-NITROBENZYL) PYRIDINE
DETECTION OF EPOXIDES WITH 4-(PARA-NITROBENZYL) PYRIDINE
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DOI：
10.1007/bf01770049
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发表时间：
1979-01-01
影响因子：
2.7
通讯作者：
KNEIP, TJ
中科院分区：
文献类型：
--
作者：
AGARWAL, SC;VANDUUREN, BL;KNEIP, TJ
材料和方法化学品。环氧化物从商业来源获得或根据文献程序合成。通过在0.4 mL乙二醇中加热80 mg NBP，然后冷却至室温，制备20%试剂溶液。将待测化合物在0.加入1 mL丙酮，然后加入0.2 mL O. 2M tris-HCl
MATERIALS AND METHODSChemicals. Epoxides were obtained from commercial sources or synthesized according to the literature procedures.Procedure. A 20% solution of the reagent was prepared by warming 80 mg NBP in 0.4 mL ethylene glycol and then cooling to room temperature. A solution of the compound to be tested in 0. I mL acetone was added followed by 0.2 mL O. 2M tris-HCl