Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion
Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion
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DOI：
10.1039/c5cc09685e
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发表时间：
2016-01-01
影响因子：
4.9
通讯作者：
Abbott, A. P.
中科院分区：
文献类型：
--
作者：
Crawford, D. E.;Wright, L. A.;Abbott, A. P.
机械化学合成已应用于通过双螺杆挤出（TSE）以连续流动方法快速合成深共晶溶剂（DES），包括Reline 200（氯化胆碱：尿素，1：2）。这得到了更高纯度的产品，时空产率（STY）比分批方法高四个数量级。
Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods.