PESTICIDE RESIDUE EVALUATION IN MAJOR STAPLE FOOD ITEMS OF ETHIOPIA USING THE QUECHERS METHOD: A CASE STUDY FROM THE JIMMA ZONE
PESTICIDE RESIDUE EVALUATION IN MAJOR STAPLE FOOD ITEMS OF ETHIOPIA USING THE QUECHERS METHOD: A CASE STUDY FROM THE JIMMA ZONE
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DOI：
10.1002/etc.2554
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发表时间：
2014-06-01
影响因子：
4.1
通讯作者：
Spanoghe, Pieter
中科院分区：
文献类型：
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作者：
Mekonen, Seblework;Ambelu, Argaw;Spanoghe, Pieter
玉米、画眉草、红辣椒和咖啡（绿色豆和带果肉的咖啡豆）的样品从埃塞俄比亚Jimma区的当地市场收集。分析了样品中氯氰菊酯、氯菊酯、溴氰菊酯、毒死蜱、二硫代氨基甲苯及其代谢物和硫丹的含量（，）。在分析方法中，采用QuEChERS（快速、简单、廉价、有效、坚固和安全）萃取方法和分散固相萃取净化（d-SPE）技术。QuEChERS方法的验证令人满意。大多数农药的回收率在70%~ 120%之间，重复性好（%相对标准偏差
Samples of maize, teff, red pepper, and coffee (green bean and coffee bean with pulp) were collected from a local market in the Jimma Zone, Ethiopia. Samples were analyzed for the occurrence of cypermethrin, permethrin, deltamethrin, chlorpyrifos ethyl, DTT and its metabolites, and endosulfan (, ). In the analytical procedure, the QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) extraction methodology with dispersive solid phase extraction clean up (d-SPE) technique was applied. Validation of the QuEChERS method was satisfactory. Recovery percentages of most pesticides were in the range of 70% to 120%, with good repeatability (%relative standard deviation