"Perfecting" WATERGATE: clean proton NMR spectra from aqueous solution
"Perfecting" WATERGATE: clean proton NMR spectra from aqueous solution
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DOI：
10.1039/c2cc37579f
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发表时间：
2013-01-01
影响因子：
4.9
通讯作者：
Morris, Gareth A.
中科院分区：
文献类型：
--
作者：
Adams, Ralph W.;Holroyd, Chloe M.;Morris, Gareth A.
对水门溶剂抑制方法的简单改进大大提高了从H2O样品中获得的H-1核磁共振光谱的质量。新方法允许H-1信号被测量，即使化学位移接近水的信号，例如碳水化合物的核磁共振光谱。
A simple modification of the WATERGATE solvent suppression method greatly improves the quality of H-1 NMR spectra obtainable from samples in H2O. The new method allows H-1 signals to be measured even when close in chemical shift to the signal of water, as for example in the NMR spectra of carbohydrates.