EBSD und STEM an hochgradig plastisch verformten Aluminiumlegierungen
EBSD und STEM an hochgradig plastisch verformten Aluminiumlegierungen
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EBSD 和 STEM 和高梯度塑料版本铝合法
DOI：
10.3139/147.110111
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发表时间：
2011
期刊：
影响因子：
--
通讯作者：
T. Lampke
中科院分区：
文献类型：
--
作者：
D. Dietrich;H. Berek;A. Schulze;Ingolf Scharf;T. Lampke
摘要铝合金经过剧烈塑性变形后，晶粒细化程度如何，是人们感兴趣的问题，而晶粒细化程度的大小取决于背散射电子衍射在横向分辨率上测得的取向数据。后向散射衍射的质量取决于成功分度的分数，这以适当的表面准备为前提。振动抛光导致基体几乎没有变形和沉淀物的优异整平，而这些相的浮雕形成（经常发生在氧化物抛光中）和溶解（经常发生在电抛光中）将降低带对比度和分度质量。因此，从背散射电子衍射得到的结果是由透射扫描电子显微镜图像支持。
Abstract After aluminum alloys undergo severe plastic deformation there is an interest in what grain refining is obtained and is determined from the orientation data detected from backscatter electron diffraction in lateral resolution. The quality of backscatter diffraction depends on the fraction of successful indexings, which presupposes an appropriate preparation of the surface. Vibration polishing results in a matrix nearly free of deformation and excellent levelling of the precipitates whereas relief formation (often occurring in oxide polishing) and dissolution (often occurring in electro-polishing) of those phases will reduce the band contrast and indexing quality. The results thus obtained from backscatter electron diffraction are backed by scanning electron microscopy images in transmission.
DOI：
10.1016/j.msea.2008.02.051
发表时间：
2009-03-15
影响因子：
6.4
作者：
Hockauf, M.;Meyer, L. W.;Krueger, L.
通讯作者：
Krueger, L.