3D Electron Diffraction for Chemical Analysis: Instrumentation Developments and Innovative Applications.

3D Electron Diffraction for Chemical Analysis: Instrumentation Developments and Innovative Applications.
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用于化学分析的三维电子衍射:仪器开发和创新应用。

DOI:
10.1021/acs.chemrev.1c00207
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发表时间:
2021-10-13
期刊:
影响因子:
62.1
通讯作者:
Mugnaioli E
Mugnaioli E
中科院分区:
化学1区
文献类型:
--
作者:
Gruene T;Mugnaioli E

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在过去的几年里,许多令人兴奋的论文报道了基于电子衍射晶体结构测定的结果。这篇综述的目的是为有兴趣进入这一新兴领域的结构化学家提供一般和实用的信息。我们讨论的技术特点,电子显微镜的研究单位,希望获得自己的仪器,以及那些实际的方面,出现不同的X射线和电子晶体学。我们还包括一个关于应用的讨论,其中电子晶体学提供的信息是不同的,可能是互补的,相对于什么是从X射线晶体学。
In the past few years, many exciting papers reported results based on crystal structure determination by electron diffraction. The aim of this review is to provide general and practical information to structural chemists interested in stepping into this emerging field. We discuss technical characteristics of electron microscopes for research units that would like to acquire their own instrumentation, as well as those practical aspects that appear different between X-ray and electron crystallography. We also include a discussion about applications where electron crystallography provides information that is different, and possibly complementary, with respect to what is available from X-ray crystallography.
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