Furnace for Inelastic X‐Ray Scattering from Liquids up to 1600°C
Furnace for Inelastic X‐Ray Scattering from Liquids up to 1600°C
复制标题
用于温度高达 1600°C 的液体非弹性 X 射线散射的炉
DOI：
10.1002/pssb.202000093
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发表时间：
2020
期刊：
影响因子：
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通讯作者：
Hattori Yasunori
中科院分区：
文献类型：
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作者：
Baron Alfred Q. R.;Inui Masanori;Ishikawa Daisuke;Matsuda Kazuhiro;Kajihara Yukio;Nakajima Yoichi;Taguchi Kazuhiko;Hattori Yasunori
描述了一种用于样品温度高达1600 °C的液体非弹性X射线散射的炉的设计和实现。在真空中工作的碳复合加热器提供了坚固的加热元件：一对加热器已在1500 °C以上的工作时间内使用超过18天，包括8个循环到室温。在1560 °C下，样品的散射角在2θ方向低至7 mrad（Q< 1 nm− 1，25.7 keV），获得了高质量的数据。
The design and implementation of a furnace for inelastic X‐ray scattering from liquids with sample temperatures up to ≈1600 °C is described. Carbon composite heaters operating in vacuum provide robust heating elements: one pair of heaters has been used for >18 days of operational time above 1500 °C, including eight cycles to room temperature. High‐quality data are obtained to scattering angles as low as 7 mrad in 2θ(Q< 1 nm−1at 25.7 keV) from a sample at 1560 °C.