Synthesis of S-aryl/alkyl thiolcarbonates from disulfides and chloroformates in the presence of the Zn/AlCl3 system
Synthesis of S-aryl/alkyl thiolcarbonates from disulfides and chloroformates in the presence of the Zn/AlCl3 system
复制标题
DOI：
10.1007/s00706-007-0778-z
复制
发表时间：
2008-03-01
影响因子：
1.8
通讯作者：
Tavoosi, Maryam
中科院分区：
文献类型：
--
作者：
Movassagh, Barahman;Tavoosi, Maryam
在80℃的干燥乙腈中，用Zn/AlCl3体系还原裂解S-S键，制备了一种简单、通用、高产的氯甲酸盐和二硫化物合成s -芳基/烷基- o -芳基/烷基硫代碳酸酯。
A simple, general, and high yielding method has been developed for the synthesis of S-aryl/alkyl-O-aryl/alkyl thiolcarbonates from various chloroformates and disulfides by reductive cleavage of the S-S bond with a Zn/AlCl3 system in dry acetonitrile at 80 degrees C.