Basic Gas Chromatography
Basic Gas Chromatography
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DOI：
10.1021/cen-v052n025.p016
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发表时间：
2019-08
期刊：
影响因子：
--
通讯作者：
H. Mcnair;James M. Miller
中科院分区：
文献类型：
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作者：
H. Mcnair;James M. Miller
第二版的前言。前言。致谢。1绪论。《简史》。定义。概述：优点和缺点。仪器仪表。参考资料。2仪器概述。运载气。流量控制和测量。样品进水口和取样装置。列。温度区域。探测器。数据系统公司。参考资料。3基本概念和术语。定义、术语和符号。利率理论。重新定义H.《分离的成就》。参考资料。4固定相。选择一列。气相色谱固定相的分类。液体固定相(GLC)。固体固定相(GSC)。参考资料。5个填充柱和进气口。坚实的支撑物。液体固定相。固体固定相(GSC)。气体分析。其他无机物的分析。液体样品和溶液的入口。特殊栏目。毛细管柱的升级。参考资料。6根毛细管柱和进样口。OT列的类型。不是立柱管道。OT柱的优势。列选择。毛细管进气系统。其他主题。参考资料。7个探测器。探测器的分类。探测器特性。火焰电离检测器(FID)。热导检测器(TCD)。电子捕获探测器(ECD)。其他探测器。参考资料。8定性和定量分析。定性分析。定量分析。参考资料。9程控温度。温度效应。PTGC的优点和缺点。PTGC的要求。PTGC理论。专题。参考资料。10气相色谱-质谱仪(GC-MS)。仪器仪表。历史。气质联用系统的局限性。数据分析。参考资料。11多维气相色谱。概述。多维色谱的基本原理。GCxGC与心脏切割。全面的GCxGC。与心脏切割LC xGC。全面的LCxGC。总结。参考资料。12种抽样方法。概述。液液萃取(LLE)。固液萃取法：索氏萃取法和加速溶剂萃取法。液-固萃取：固相萃取(SPE)。液体或固体蒸气萃取：顶空萃取。固相微萃取(SPME)。其他技术和摘要。参考资料。13个专题。快速GC。气相色谱手性分析。非挥发性化合物的气相色谱分析参考资料。14排除GC系统故障。附录一：符号和缩略语。附录二选择毛细管柱的准则。附录III GC：如何避免问题。附录四OT塔分流进样分流比的计算。附录五毛细管柱的操作条件。附录六OV液相物性数据。附录七部分压缩修正系数(J)。附录部分气体色谱图互联网网站。附录九关于气相色谱的其他书籍。应用程序索引。索引。
PREFACE TO THE SECOND EDITION. PREFACE. ACKNOWLEDGMENTS. 1 INTRODUCTION. A Brief History. Definitions. Overview: Advantages and Disadvantages. Instrumentation. References. 2 INSTRUMENT OVERVIEW. Carrier Gas. Flow Control and Measurement. Sample Inlets and Sampling Devices. Columns. Temperature Zones. Detectors. Data Systems. References. 3 BASIC CONCEPTS AND TERMS. Definitions, Terms, and Symbols. The Rate Theory. A Redefinition of H. The Achievement of Separation. References. 4 STATIONARY PHASES. Selecting a Column. Classification of Stationary Phases for GLC. Liquid Stationary Phases (GLC). Solid Stationary Phases (GSC). References. 5 PACKED COLUMNS AND INLETS. Solid Supports. Liquid Stationary Phases. Solid Stationary Phases (GSC). Gas Analysis. Analysis of Other Inorganics. Inlets for Liquid Samples and Solutions. Special Columns. Upgrading for Capillary Columns. References. 6 CAPILLARY COLUMNS AND INLETS. Types of OT Columns. OT Column Tubing. Advantages of OT Columns. Column Selection. Capillary Inlet Systems. Miscellaneous Topics. References. 7 DETECTORS. Classification of Detectors. Detector Characteristics. Flame Ionization Detector (FID). Thermal Conductivity Detector (TCD). Electron Capture Detector (ECD). Other Detectors. References. 8 QUALITATIVE AND QUANTITATIVE ANALYSIS. Qualitative Analysis. Quantitative Analysis. References. 9 PROGRAMMED TEMPERATURE. Temperature Effects. Advantages and Disadvantages of PTGC. Requirements of PTGC. Theory of PTGC. Special Topics. References. 10 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS). Instrumentation. History. Limitations of GC-MS Systems. Data Analysis. References. 11 MULTIDIMENSIONAL GAS CHROMATOGRAPHY. Overview. Fundamental Principles of Multidimensional Chromatography. GCxGC with Heart Cutting. Comprehensive GCxGC. LCxGC with Heart Cutting. Comprehensive LCxGC. Summary. References. 12 SAMPLING METHODS. Overview. Liquid-Liquid Extraction (LLE). Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE). Liquid-Solid Extraction: Solid-Phase Extraction (SPE). Liquid- or Solid-Vapor Extraction: Headspace Extraction. Solid-Phase Micro-extraction (SPME). Additional Techniques and Summary. References. 13 SPECIAL TOPICS. Fast GC. Chiral Analysis by GC. GC Analysis of Nonvolatile Compounds. References. 14 TROUBLESHOOTING GC SYSTEMS. APPENDIX I SYMBOLS AND ACRONYMS. APPENDIX II GUIDELINES FOR SELECTING CAPILLARY COLUMNS. APPENDIX III GC: HOW TO AVOID PROBLEMS. APPENDIX IV CALCULATION OF SPLIT RATIO FOR SPLIT INJECTION ON OT COLUMNS. APPENDIX V OPERATING CONDITIONS FOR CAPILLARY COLUMNS. APPENDIX VI OV LIQUID PHASES PHYSICAL PROPERTY DATA. APPENDIX VII SOME COMPRESSIBILITY CORRECTION FACTORS (J). APPENDIX VIII SOME INTERNET WEBSITES FOR GAS CHROMATOGRAPHERS. APPENDIX IX OTHER BOOKS ON GAS CHROMATOGRAPHY. INDEX OF APPLICATIONS. INDEX.