Growth of crystalline Sb2S3 nanorods by hydrothermal method
Growth of crystalline Sb2S3 nanorods by hydrothermal method
复制标题
水热法生长晶体 Sb2S3 纳米棒
DOI：
10.1016/s0022-0248(03)01266-1
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发表时间：
2003-08-01
影响因子：
1.8
通讯作者：
Qian, YT
中科院分区：
文献类型：
--
作者：
Li, C;Yang, XG;Qian, YT
以SbCl 3和Na 2S为原料，在180 ℃下水热12 h，制备了结晶的硫化锑（Sb 2S 3）纳米棒。X射线粉末衍射（XRD）分析表明，所制备的纳米棒为正交相Sb 2S 3，晶格参数a = 11.22埃，B = 11.28埃，c = 3.84埃。透射电子显微镜（TEM）显示所制备的Sb_2S_3为直径为30- 100 nm、长度为0.3-5 μ m的结晶纳米棒。研究了各种因素对纳米棒生长的影响。讨论了可能的生长过程。(C)出版社：Elsevier Science B. V.
Crystalline antimony sulfide (Sb2S3) nanorods were hydrothermally prepared starting from SbCl3 and Na2S at 180degreesC for 12h. X-ray powder diffraction (XRD) showed that the as-prepared nanorods were orthorhombic-phase Sb2S3 with lattice parameters a = 11.22Angstrom, b = 11.28Angstrom, c = 3.84Angstrom. Transmission electron microscopy (TEM) showed that the as-prepared Sb2S3 are crystalline nanorods with a size of 30-100nm in diameter and 0.3-5 mum in length. The various effects on the growth of nanorods were studied. The possible growth process was discussed. (C) 2003 Published by Elsevier Science B.V.