Convenient synthesis of β-truxinic acid via photodimerization of p-nitrophenyl cinnamate in the crystalline state

Convenient synthesis of β-truxinic acid via photodimerization of p-nitrophenyl cinnamate in the crystalline state
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通过晶态对硝基苯肉桂酸酯的光二聚化方便合成 β-truxinic 酸

DOI:
10.1246/bcsj.58.3399
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发表时间:
1985
影响因子:
4
通讯作者:
T. Iizawa
T. Iizawa
中科院分区:
化学3区
文献类型:
--
作者:
T. Nishikubo;E. Takahashi;Takatoshi Miyaji;T. Iizawa

文献摘要

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通过对-硝基肉桂酸苯酯晶体的光致化学二聚,然后对得到的二聚体进行水解,以极高的产率合成了β-特鲁辛酸。
β-Truxinic acid was synthesized in extremely high yield via a topochemical photodimerization of p-nitrophenyl cinnamate crystals, followed by the hydrolysis of the obtained dimer.