Stress singularity near the crack-tip in silicon carbide : Investigation by atomic force microscopy

Stress singularity near the crack-tip in silicon carbide : Investigation by atomic force microscopy
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碳化硅裂纹尖端附近的应力奇点:原子力显微镜研究

DOI:
10.1016/s1359-6454(98)00076-7
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发表时间:
1998
期刊:
影响因子:
9.4
通讯作者:
T. Kinoshita
T. Kinoshita
中科院分区:
材料科学1区
文献类型:
--
作者:
T. Kinoshita

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利用原子力显微镜(AFM)的高空间分辨率,发展了一种新的尖端应力场测量技术。为了评估所提出的技术的灵敏度,近尖端应力奇异性在98 N努氏裂纹热压碳化硅进行了研究,在弯曲过程中的应力为110 MPa的原位AFM观察。AFM观察得到的形貌表明,近端应力奇异性产生了长轴为1.20 μm的椭圆形中空区域。垂直位移在裂纹尖端附近最大,最大值为2.5nm。进行了三维有限元(FEM)分析,得到的位移与原子力显微镜测量的位移一致。通过对AFM形貌的分析,验证了裂纹尖端的应力场可以被评估,并且AFM测量的凹陷源于应力奇异性。
A new technique using the high spatial resolution of atomic force microscopy (AFM) was developed to measure the near-tip stress field. In order to assess the sensitivity of the proposed technique, the near-tip stress singularity at a 98 N Knoop crack in hot-pressed silicon carbide was investigated by in situ AFM observations during bending with a stress of 110 MPa. The topographies obtained in the AFM observations indicated that the near-tip stress singularity produced an elliptical hollow area with a long axis of ∼20μm. The vertical displacement was highest near the crack-tip with a maximum of 2.5nm. Three-dimensional finite-element (FEM) analyses were performed and the displacements obtained were consistent with those measured by AFM. It was verified that the crack-tip stress field can be evaluated by analyzing the AFM topographies and that the depression measured by AFM originates in the stress singularity.
DOI: 10.1016/0013-7944(81)90116-8
发表时间: 1981-01-01
影响因子: 5.4
作者:
NEWMAN, JC;RAJU, IS
通讯作者: RAJU, IS