Achievement of 1H-19F heteronuclear experiments using the conventional spectrometer with a shared single high band amplifier
Achievement of 1H-19F heteronuclear experiments using the conventional spectrometer with a shared single high band amplifier
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使用具有共享单个高频带放大器的传统光谱仪完成 1H-19F 异核实验
DOI：
10.1002/mrc.4210
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发表时间：
2015
期刊：
影响因子：
--
通讯作者：
Kazuo Furihata and Mitsuru Tashiro
中科院分区：
文献类型：
--
作者：
Chiseko Sakuma;Jun-ichi Kurita;Kazuo Furihata and Mitsuru Tashiro
1H-19 F杂波NMR实验使用配备有单个高频带放大器和1H/19 F/13 C双调谐探针的常规光谱仪来实现。虽然通常需要双高带放大器来进行这样的实验，但在常规谱仪中简单地修改路径就能够获得各种1H-19 F杂散谱。本技术的效率被证明在19 F {1H}和1H {19 F}饱和转移差异实验的应用。版权所有© 2015约翰威利父子有限公司.
The1H–19F heteronuclear NMR experiments were achieved using the conventional spectrometer equipped with a single high band amplifier and a1H/19F/13C double‐tuned probe. Although double high band amplifiers are generally required to perform such experiments, a simple modification of pathway in the conventional spectrometer was capable of acquiring various1H–19F heteronuclear spectra. The efficiency of the present technique was demonstrated in an application for19F{1H} and1H{19F} saturation transfer difference experiments. Copyright © 2015 John Wiley & Sons, Ltd.