Simultaneous determination of melamine and related compounds by capillary zone electrophoresis
Simultaneous determination of melamine and related compounds by capillary zone electrophoresis
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毛细管区带电泳法同时测定三聚氰胺及相关化合物
DOI：
10.1016/j.foodcont.2009.12.009
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发表时间：
2010-06
期刊：
影响因子：
6
通讯作者：
Shouzhuo Yao
中科院分区：
文献类型：
--
作者：
Jingen Xia;Naiyuan Zhou;Yujun Liu;Bo Chen;Yongning Wu;Shouzhuo Yao
A simple, rapid and accurate method for the simultaneous determination of melamine and related compounds (ammeline, ammelide and cyanuric acid) by capillary zone electrophoresis with diode array detection (CZE–DAD) was developed and successfully applied in egg, dairy products and pet feed. Real samples were extracted with acetonitrile/water/diethylamine (80/18/2, v/v/v) and analyzed by CZE method directly after centrifuging and filtering. Separation was performed by CZE using 40mM disodium hydrogen phosphate buffer (pH 9.0) as running buffer, an applied voltage of +30kV, and UV detection at 214nm. Four targets were separated completely within 10min. The optimized method demonstrated good performance concerning linearity (r⩾0.9964), precision (⩽4%), accuracy (82.2–101.6%), and enough sensitivity. And the proposed method was proved to have the merits of good separation, easy operation, short analysis time and low cost.
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影响因子：
4.1
作者：
V. Pichon;L. Chen;S. Guenu;M. Hennion
通讯作者：
V. Pichon;L. Chen;S. Guenu;M. Hennion
DOI：
10.1007/bf00527969
发表时间：
1968-07
期刊：
Fresenius' Zeitschrift für analytische Chemie
影响因子：
--
作者：
R. Bacaloglu;C. Csunderlik;G. Ostrogovich
通讯作者：
R. Bacaloglu;C. Csunderlik;G. Ostrogovich
影响因子：
6.1
作者：
Filigenzi, Michael S.;Puschner, Birgit;Poppenga, Robert H.
通讯作者：
Poppenga, Robert H.
DOI：
--
发表时间：
2009
期刊：
Lc Gc North America
影响因子：
--
作者：
Eugene Chang;D. Ji;R. Arora
通讯作者：
Eugene Chang;D. Ji;R. Arora
影响因子：
2.7
作者：
T. Sugita;H. Ishiwata;K. Yoshihira;A. Maekawa
通讯作者：
T. Sugita;H. Ishiwata;K. Yoshihira;A. Maekawa