FACILE PRODUCT ISOLATION FROM ORGANO-STANNANE REDUCTIONS OF ORGANIC HALIDES
FACILE PRODUCT ISOLATION FROM ORGANO-STANNANE REDUCTIONS OF ORGANIC HALIDES
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DOI：
10.1021/jo01317a032
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发表时间：
1979-01-01
影响因子：
3.6
通讯作者：
JACOBUS, J
中科院分区：
文献类型：
--
作者：
LEIBNER, JE;JACOBUS, J
The reduction of organic halides by organostannanes, first reported by vanderKerk et al., 2 has subsequently found nu-merous applications. The reduction product has generally been separated from the organotin halide byproduct by dis-tillation, gas chromatography, selective extraction, column chromatography, sublimation, a combination of some of these techniques, or in an unspecified manner. 3 We would like to report a facile, general method for the isolation of reduction products from the concomitantly formed organotin halide byproducts (eq 1).
