Raman Studies of ZnO Products Synthesized by Solution Based Methods
Raman Studies of ZnO Products Synthesized by Solution Based Methods
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基于溶液的方法合成 ZnO 产品的拉曼研究
DOI：
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发表时间：
2016
期刊：
影响因子：
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通讯作者：
H. Akbulut
中科院分区：
文献类型：
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作者：
D. Gultekin;H. Akbulut
在这项研究中，纳米结构的ZnO薄膜涂层的溶胶-凝胶法生产已检查和表征。以二水合醋酸锌（Zn（CH 3COO）2 ·2 H2O）为前驱体，在液相中制备ZnO溶胶，制备了ZnO薄膜涂层。乙醇（C2 H5 OH）已被用作溶剂材料，单乙醇胺（MEA）已被用作络合剂。最终溶液具有0.1、0.3、0.5、0.7和1摩尔浓度。利用扫描电子显微镜（SEM）对样品的形貌和结构进行了表征。使用X射线衍射（XRD）和拉曼光谱对合成的涂层进行定性分析。对前驱体、溶液和最终产物进行了拉曼光谱研究，以研究化合物从初始材料到最终涂层的转化。
In this study, nanostructured ZnO thin film coatings produced by sol-gel method have been examined and characterized. ZnO thin film coatings synthesized by the preparation of ZnO sols in the liquid phase from homogeneous solutions with precursor of zinc acetate dihydrate (Zn(CH3COO)2 ·2H2O). Ethanol (C2H5OH) has been used as a solvent material and monoethanolamine (MEA) has been used as a complexing agent. The final solutions have 0.1, 0.3, 0.5, 0.7 and 1 molar concentrations. General morphologies and detailed structural characterizations have been obtained by using scanning electron microscope (SEM). Qualitative analyses of the synthesized coatings were performed using X-ray diffraction (XRD) and Raman spectroscopy. The Raman spectroscopy studies of precursor, solution and final products were carried out to investigate transformation of the chemical compounds from the initial material to the final coating.