Rapid direct determination of organic carbon and nitrogen in carbonate‐bearing sediments with a Yanaco MT‐5 CHN analyzer
Rapid direct determination of organic carbon and nitrogen in carbonate‐bearing sediments with a Yanaco MT‐5 CHN analyzer
复制标题
DOI:
10.4319/lo.1995.40.5.1001
复制
发表时间:
1995-07
影响因子:
4.5
通讯作者:
M. Yamamuro;H. Kayanne
中科院分区:
文献类型:
--
作者:
M. Yamamuro;H. Kayanne
A rapid technique is presented for measuring organic C and N in carbonate-bearing sediments. Organic C and N were determined with a Yanaco MT-5 CHN analyzer after removing carbonate by acidification of samples in ceramic sample boats with HCI vapor. This procedure eliminates loss of acid-soluble organic matter during carbonate dissolution. The accuracy of this new technique and two earlier methods of determining organic C and N concentrations was verified with standard chemicals and carbonate-bearing sediments (>80 wt% CaCO 3 ). With the new technique there was no contamination or loss of organic C and N. The method is suitable for acidifying sediments with a wide range of carbonate content.