HYDROTHERMAL GROWTH OF LARGE SOUND CRYSTALS OF ZINC OXIDE

HYDROTHERMAL GROWTH OF LARGE SOUND CRYSTALS OF ZINC OXIDE
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DOI:
10.1111/j.1151-2916.1964.tb14632.x
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发表时间:
1964-01-01
影响因子:
3.9
通讯作者:
CAPORASO, AJ
CAPORASO, AJ
中科院分区:
材料科学2区
文献类型:
--
作者:
LAUDISE, RA;KOLB, ED;CAPORASO, AJ

文献摘要

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大(10至20克)宏观上健全的ZnO晶体适合于初步的传感器和其他研究已经生长水热速率从10至15密耳每天。发现在实现良好生长中重要的因素是(1)生长溶液的基浓度,(2)溶解和生长区域之间的温差,(3)生长溶液的预饱和,(4)预热程序,(5)向生长溶液中添加Li+以抑制枝晶形成,(6)蚀刻以去除种子损伤,以及(7)营养物尺寸。对上述每一个因素都进行了研究和讨论。
Large (10 to 20 g) macroscopically sound ZnO crystals suitable for preliminary transducer and other studies have been grown hydrothermally at rates of from 10 to 15 mils per day. The factors found to be important in achieving good growth were (1) base concentration of growth solution, (2) temperature difference between dissolving and growth regions, (3) presaturation of growth solution, (4) warm‐up procedure, (5) addition of Li+ to the growth solution to suppress dendrite formation, (6) etching to remove seed damage, and (7) nutrient size. Each of the foregoing factors was studied and is discussed.