Round robin testing of a percolation column leaching procedure.
Round robin testing of a percolation column leaching procedure.
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渗滤柱浸出程序的循环测试。
DOI：
10.1016/j.wasman.2016.06.010
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发表时间：
2016
期刊：
影响因子：
8.1
通讯作者：
Luc Debaene
中科院分区：
文献类型：
--
作者：
Roeland Geurts;J. Spooren;M. Quaghebeur;K. Broos;Cindy Kenis;Luc Debaene
循环试验结果的渗滤柱浸出程序（CEN/TS 14405：2004），由佛兰芒技术研究所（VITO）组织，在13年的时间跨度与8和18个不同的实验室之间的参与和讨论。重点是重金属砷，镉，铬，铜，汞，镍，铅和锌从矿物废料的可吸收性。通过对获得的结果进行统计分析，可以深入了解色谱柱沥滤试验的再现性和重复性。实验室内和实验室间的变异性之比为1：3。洗脱液中元素浓度的重现性在元素、材料和组分（即不同的液固比）之间存在显著差异。的重现性进行了讨论，在光的应用程序中的柱浸出试验的法律的和环境政策的目的。此外，还对实验室的性能进行了比较。
Round robin test results of a percolation column leaching procedure (CEN/TS 14405:2004), organised by the Flemish Institute for Technological Research (VITO), over a time span of 13 years with a participation of between 8 and 18 different laboratories are presented and discussed. Focus is on the leachability of heavy metals As, Cd, Cr, Cu, Hg, Ni, Pb and Zn from mineral waste materials. By performing statistical analyses on the obtained results, insight into the reproducibility and repeatability of the column leaching test is gathered. A ratio of 1:3 between intra- and inter-laboratory variability is found. The reproducibility of the eluates’ element concentrations differ significantly between elements, materials and fractions (i.e. different liquid-to-solid ratios). The reproducibility is discussed in light of the application of the column leaching test for legal and environmental policy purposes. In addition, the performances of laboratories are compared.