Cuprous oxide nanowires prepared by an additive-free polyol process
Cuprous oxide nanowires prepared by an additive-free polyol process
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DOI：
10.1021/cg060615t
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发表时间：
2007-02-01
影响因子：
3.8
通讯作者：
Zigon, Majda
中科院分区：
文献类型：
--
作者：
Orel, Zorica Crnjak;Anzlovar, Alojz;Zigon, Majda
首次采用多元醇法制备了氧化亚铜纳米线，其前驱体为一水乙酸铜和二甘醇（DEG）。在控制反应温度（190℃）、前驱体浓度（0.01 ~ 0.1 mol/L）和反应时间（6 h）的条件下，制备了直径约为20 nm、长度可达5 μ m的Cu2O纳米线，并用SEM、TEM、XRD和IR对其进行了表征。
The polyol method was employed for the first time to synthesize cuprous oxide nanowires using only a precursor of Cu(II) acetate monohydrate and diethylene glycol (DEG). With careful control of the reaction temperature (190 degrees C), the precursor concentration (0.01-0.1 mol/L), and the reaction time (6 h), we prepared Cu2O nanowires with a diameter of approximately 20 nm and a length up to 5 mu m. The nanowires were characterized by SEM, TEM, XRD, and IR spectroscopy.