A method to stabilize the incident X-ray energy for anomalous diffraction measurements

A method to stabilize the incident X-ray energy for anomalous diffraction measurements
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一种稳定异常衍射测量的入射 X 射线能量的方法

DOI:
10.1107/s1600577517006312
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发表时间:
2017
影响因子:
2.5
通讯作者:
Liu Peng
Liu Peng
中科院分区:
物理与天体物理3区
文献类型:
--
作者:
Wang Wenjia;Yang Xiaoyun;Chang Guangcai;An Pengfei;Cha Kewen;Dong Yuhui;Liu Peng

文献摘要

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本文提出了一种用于异常衍射数据采集的X射线入射能量的标定和稳定方法,并成功地应用于北京同步辐射装置单晶衍射光束线1W2B上。该方法采用反馈回路控制双晶单色器的运动,使入射X射线能量在吸收边拐点处保持在0.2eV范围内。 
A method to calibrate and stabilize the incident X-ray energy for anomalous diffraction data collection is provided and has been successfully used at the single-crystal diffraction beamline 1W2B at the Beijing Synchrotron Radiation Facilities. Employing a feedback loop to control the movement of the double-crystal monochromator, this new method enables the incident X-ray energy to be kept within a 0.2 eV range at the inflection point of the absorption edge.