X-ray diffraction and pycnometric determinations of the density of zirconium-base interstitial phases
X-ray diffraction and pycnometric determinations of the density of zirconium-base interstitial phases
复制标题
锆基间隙相密度的 X 射线衍射和比重测定
DOI：
10.1007/bf00796955
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发表时间：
1970
期刊：
影响因子：
--
通讯作者：
R. A. Lyutikov
中科院分区：
文献类型：
--
作者：
A. Shevchenko;R. A. Andrievskii;V. P. Kalinin;R. A. Lyutikov
制备研究物质的起始材料是电解锆粉。*在氮化物的制备中，该粉末在1300-1800℃的温度下用高纯氮气浸渍，在700-900℃下进行氢气浸渍。通过将锆粉和光谱纯石墨在10-6毫米汞柱（1700和1700℃）的真空中进行两阶段合成，获得碳化物。 2000~ 中间研磨）。以Zr-ZrN和Zr-ZrC混合物为原料，在900-1000~900℃的氢气气氛中合成了三元化合物。
The starting material for the preparation of substances for investigation was an electrolytic zirconium powder.* In the preparation of nitrides, this powder was impregnated with high-purity nitrogen at temperatures of 1300-1800~ Impregnation with hydrogen was effected at 700-900~ Carbides were obtained by subjecting the zirconium powder and spectral-purity graphite to two-stage synthesis in a vacuum of 10-6 mm Hg (1700 and 2000~ with intermediate grinding). Ternary compounds were synthesized from Zr-ZrN and Zr-ZrC mixtures in a hydrogen atmosphere at 900-1000~