WO3 nanorods/nanobelts synthesized via physical vapor deposition process

WO3 nanorods/nanobelts synthesized via physical vapor deposition process
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DOI:
10.1016/s0009-2614(02)01702-5
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发表时间:
2003-01-02
影响因子:
2.8
通讯作者:
Kurashima, K
Kurashima, K
中科院分区:
化学4区
文献类型:
--
作者:
Li, YB;Bando, Y;Kurashima, K

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采用简单的物理气相沉积技术,在950-1000 ℃的空气中,氧化钨丝,通过红外辐射加热原位蒸发,在Si基片上制备了WO 3一维纳米结构。大多数纳米结构是具有多边形横截面的纳米棒,宽度为数十纳米。纳米棒为单晶单斜结构,轴向沿[1 0 0]或[0 1 0]方向沿着。此外,还形成了一些六方结构的单晶纳米带,其长度方向沿着[1 1 0]方向。根据它们的晶胞参数讨论了两种不同结构的形成。(C)2002 Elsevier Science B. V.保留所有权利。
A simple physical vapor deposition technique, oxidizing W filaments and in situ evaporating via infrared irradiation heating at 950-1000 degreesC in air, was developed to prepare WO3 one-dimensional nanostructures on Si wafers. Most of the nanostructures were nanorods with polygonal cross-sections, tens of nanometers in width. The nanorods were single-crystalline monoclinic structure, with the axes preferentially aligned along the [1 0 0] or [0 1 0] directions. In addition, some single-crystalline nanobelts of hexagonal structure were formed, with their length directions lying along the [1 1 0] direction. The formation of two different structures is discussed based on their cell parameters. (C) 2002 Elsevier Science B.V. All rights reserved.