STEM imaging of 47-pm-separated atomic columns by a spherical aberration-corrected electron microscope with a 300-kV cold field emission gun

STEM imaging of 47-pm-separated atomic columns by a spherical aberration-corrected electron microscope with a 300-kV cold field emission gun
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DOI:
10.1093/jmicro/dfp030
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发表时间:
2009-12-01
期刊:
JOURNAL OF ELECTRON MICROSCOPY
影响因子:
--
通讯作者:
Takayanagi, Kunio
Takayanagi, Kunio
中科院分区:
其他
文献类型:
--
作者:
Sawada, Hidetaka;Tanishiro, Yasumasa;Takayanagi, Kunio

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最近研制了一种球差校正的电子显微镜,它配备了300千伏的冷场发射枪和一个色差系数较小的物镜。在高角环形暗场(HAADF)扫描透射式电子显微镜(STEM)中,用0.4 eV的电子束能量扩展分辨出间隔为47 pm的哑铃图像,该哑铃图像对应于沿[114]方向排列的一对Ge原子柱。将观测图像与动力学计算得到的模拟图像进行了比较。
A spherical aberration-corrected electron microscope has been developed recently, which is equipped with a 300-kV cold field emission gun and an objective lens of a small chromatic aberration coefficient. A dumbbell image of 47 pm spacing, corresponding to a pair of atomic columns of germanium aligned along the [114] direction, is resolved in high-angle annular dark field (HAADF) scanning transmission electron microscopy (STEM) with a 0.4-eV energy spread of the electron beam. The observed image was compared with a simulated image obtained by dynamical calculation.