Generation and characterization of zirconium nitride nanoparticles by wire explosion process

Generation and characterization of zirconium nitride nanoparticles by wire explosion process
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DOI:
10.1016/j.ceramint.2012.03.065
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发表时间:
2012-09
影响因子:
5.2
通讯作者:
R. S. Reddy;M. Kamaraj;U. Mudali;S. Chakravarthy;R. Sarathi
R. S. Reddy;M. Kamaraj;U. Mudali;S. Chakravarthy;R. Sarathi
中科院分区:
材料科学1区
文献类型:
--
作者:
R. S. Reddy;M. Kamaraj;U. Mudali;S. Chakravarthy;R. Sarathi

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本文采用线爆法制备了氮化锆纳米颗粒。通过X射线衍射(XRD)和选区电子衍射(SAED)研究,其特征在于所产生的ZrN纳米粒子。使用透射电子显微镜(TEM)分析颗粒的尺寸和形状。使用基于对数正态概率分布的分析来量化粉末的粒度分布。采用高速摄影技术对电爆过程进行了观察。
In the present study, wire explosion process (WEP) has been used to produce zirconium nitride (ZrN) nanoparticles. The produced ZrN nanoparticles were characterized through X-ray diffraction (XRD) and by the selected area electron diffraction (SAED) studies. The size and shape of the particles were analyzed using Transmission Electron Microscope (TEM). An analysis based on Log-normal probability distribution was used to quantify the particle size distribution of the powder. High speed photography was used to observe the wire explosion process.