Facile fabrication of long α-Fe 2O 3, α-Fe and γ-Fe 2O 3 hollow fibers using sol–gel combined co-electrospinning technology
Facile fabrication of long α-Fe 2O 3, α-Fe and γ-Fe 2O 3 hollow fibers using sol–gel combined co-electrospinning technology
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DOI:
10.1016/j.jcis.2006.12.026
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发表时间:
2007-04
影响因子:
9.9
通讯作者:
Sihui Zhan;Dairong Chen;X. Jiao;Shusheng Liu
中科院分区:
文献类型:
--
作者:
Sihui Zhan;Dairong Chen;X. Jiao;Shusheng Liu
Long α-Fe2O3hollow fibers have been prepared through a facile sol–gel combined co-electrospinning technique using ferric citrate as precursor, and α-Fe and γ-Fe2O3hollow fibers have been obtained by reduction and reoxidation at different conditions. The outer diameter of the as-prepared hollow fibers is 0.5–5 μm with wall thickness of 200–800 nm. The obtained tubular fibers were characterized by thermal gravimetric (TG), FT-IR spectra, X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and Raman techniques. In addition, magnetic properties of α-Fe and γ-Fe2O3hollow fibers have also been investigated.